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Microstructure and mechanical properties of a commercially pure Ti processed by warm equal channel angular pressing

机译:通过等通道角挤压加工的商业纯Ti的微观结构和机械性能

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摘要

A commercially pure (CP) Titanium alloy classified as Grade 1, was processed by Equal Channel Angular Pressing (ECAP) up to 4 passes in the temperature range of 450-150 degrees C.; The resulting microstructures were observed by Electron Back-Scattered Diffraction, revealing a bimodal grain size distribution consisting of small recrystallized grains of submicrometer size, with an average value of 0.3 mu m, and elongated bands of 1.4 mu m with different degree of substructure. Additionally the fraction of restored and deformed grains were evaluated as a function of processing temperature following an internal grain misorientation criterion, leading to an overall fraction of recrystallized grains between 40% and 20% in samples ECAPed at 450 and 150 degrees C, respectively.; The strengthening contributions of the grain size, equivalent oxygen content (O-eq) and Low Angle Grain Boundaries (LAGBs) to the yield stress were identified by the Hall Fetch and Taylor equations. The strengthening coefficient k of the Hall-Fetch relation was approximately 5 MPa mm(-1/2), with an increment of 0.44 MPa mm(-1/2) per 0.1 O-eq.-%, while the LAGB strengthening contribution was responsible approximately by half of the experimental yield stress values measured. (C) 2014 Elsevier B.V. All rights reserved.
机译:通过等通道角挤压(ECAP)在450-150摄氏度的温度范围内进行了多达4道次加工的商业纯净(CP)钛合金,分类为1级;通过电子背散射衍射观察所得的微结构,揭示了双峰晶粒尺寸分布,其由亚微米尺寸的小再结晶晶粒组成,平均粒径为0.3μm,具有1.4μm的细长带,具有不同的亚结构度。另外,根据内部晶粒取向错误的标准,根据加工温度对还原和变形晶粒的分数进行了评估,结果分别在450和150℃ECAP下得到的样品中再结晶晶粒的总分数在40%和20%之间。晶粒尺寸,当量氧含量(O-eq)和低角度晶粒边界(LAGBs)对屈服应力的增强作用由Hall Fetch和Taylor方程确定。 Hall-Fetch关系的强化系数k约为5 MPa mm(-1/2),每0.1 Oeq-%增加0.44 MPa mm(-1/2),而LAGB强化贡献为大约是所测得的实验屈服应力值的一半。 (C)2014 Elsevier B.V.保留所有权利。

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